HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 11749027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | (2S,3S)-1,2-Epoxy-3-(Cbz-amino)-4-phenylbutane | HCID 9861019 | — |
| Product | HCID 11749027 | HCID 11749027 | 81% |
Reaction Steps
Part A: From the reaction of (1.48 g, 5.0 mmol) of N-benzyloxycarbonyl 3(S)-amino-1,2-(S)-epoxy-4-phenylbutane and (7.314 g, 100.0 mmol) of n-butylamine, one obtains 1.50 g (80%) of N-[3(S)-benzyloxycarbonylamino-2(R)-hydroxy-4-phenylbutyl]-N-butylamine, mp 125°-128° C., FAB MS, Spectrum: MH+ =371.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705500 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-c2d28342d34642209e1e35c2a0a60d19 |
| Source note | uspto-grants-1998_01 |