HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylparaben → HCID 470684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylparaben | HCID 7456 | — |
| Reactant | 2-chloro-8-chloromethyl-5,11-dihydro-11-ethyl-5-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one | HCID 10830738 | — |
| Product | HCID 470684 | HCID 470684 | 45% |
Reaction Steps
Using a procedure analogous to that described in Example 98, the title compound, m.p. 196°-197° C., was prepared from 2-chloro-8-chloromethyl5,11-dihydro-11-ethyl-5-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and methyl 4-hydroxybenzoate. The yield was 45% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705499 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-dbdfc0087b7c42a0bec61cfc80bb2beb |
| Source note | uspto-grants-1998_01 |