HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-8-chloromethyl-5,11-dihydro-11-ethyl-5-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one → HCID 470708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-8-chloromethyl-5,11-dihydro-11-ethyl-5-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one | HCID 10830738 | — |
| Reactant | pyridine-4-thiol | HCID 178418431 | — |
| Product | HCID 470708 | HCID 470708 | 79% |
Reaction Steps
Using a procedure analogous to that described in Example 117, the title compound, m.p. 140°-142° C., was prepared from 2-chloro-8-chloromethyl-5,11-dihydro-11-ethyl-5-methyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and 4-mercaptopyridine. The yield was 79% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705499 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-869c694bfcbc41b1aa788c95838b947f |
| Source note | uspto-grants-1998_01 |