HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-(6-Methyl-1H-indol-3-yl)ethan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 15274383 | HCID 15274383 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 2-(6-Methyl-1H-indol-3-yl)ethan-1-amine | HCID 190006 | — |
Reaction Steps
A sample of 6-methyl-7-bromo-1H-indole-3-ethanamine was contacted with Pd/C H2 in the presence of ethanol and triethylamine. The resulting material was evaporated and partitioned between base/CHCl3. The organic phase was dried, concentrated, and dried. The resulting material was taken up into methanol and added to ethereal HCl. The resulting material was washed and vacuum dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05705519 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-10ba96c956e94c0689d3d24e36f3db86 |
| Source note | uspto-grants-1998_01 |