Methanol → HCID 19708979, compound
Reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]2[C:10]3[N:18]=[C:17]([N:19]4[CH2:24][CH2:23][CH:22]([C:25]([OH:27])=[O:26])[CH2:21][CH2:20]4)[N:16]=[CH:15][C:11]=3[N:12]=[CH:13][N:14]=2)[CH:5]=[CH:6][CH:7]=1.S(Cl)(Cl)=O.[CH3:32]O>>[CH3:1][C:2]1[CH:3]=[C:4]([NH:8][C:9]2[C:10]3[N:18]=[C:17]([N:19]4[CH2:24][CH2:23][CH:22]([C:25]([O:27][CH3:32])=[O:26])[CH2:21][CH2:20]4)[N:16]=[CH:15][C:11]=3[N:12]=[CH:13][N:14]=2)[CH:5]=[CH:6][CH:7]=1Participants
4
Procedure
Prepared from compound 46 of Example 1 by reaction with thionyl chloride and methanol.
Sources & evidence
- ORD record
- ord-2b7c33f65d9841c6bfdea1bd48780215
- Source dataset
- uspto-grants-1998_01
- Patent number
- US05707989
Reaction notes
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