HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodobenzenesulfonyl chloride → HCID 22611599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodobenzenesulfonyl chloride | HCID 7399 | — |
| Reactant | 3-(1-Methylpiperidin-4-yl)-1h-indol-5-amine | HCID 11831220 | — |
| Product | HCID 22611599 | HCID 22611599 | — |
Reaction Steps
Following the procedure described in detail in Example 39, 0.791 gm (3.45 mMol) 5-amino-3-(1-methylpiperidin-4-yl)-1H-indole and 1.1 gm (3.62 mMol) 4-iodobenzenesulfonyl chloride were used to prepare 0.809 (47.3%) of the title compound as a white powder. m.p.>250° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05708008 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-7b10e664e0844040b8f78310708b1436 |
| Source note | uspto-grants-1998_01 |