(Chloromethyl)cyclohexane → HCID 178420897, compound

HRID 726237Notes

Reaction equation

HRID 726237 reaction equation
[CH:1]1([CH2:7]Cl)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(C(C2C=CC=CC=2)(C2C=CC=CC=2)[N:16]2[CH:20]=[C:19]([CH2:21][O-:22])[N:18]=[CH:17]2)C=CC=CC=1.[Na+]>>[NH:16]1[CH:20]=[C:19]([CH2:21][O:22][CH2:7][CH:1]2[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]2)[N:18]=[CH:17]1

Participants

3

Reactant 2

HCID 3015335(Chloromethyl)cyclohexaneHCID 67661982sodium (1-triphenylmethyl-1H-imidazol-4-yl)-methanolate

Product 1

HCID 178420897HCID 178420897, compound

Procedure

The preparation is carried out as in Example 36 with cyclohexylmethyl chloride and sodium [1-(triphenylmethyl)imidazol-4-yl]methoxide. The title compound is crystallized in the hydrogenmaleate form from ethanol/diethyl ether.

Workup

  1. customThe title compound is crystallized in the hydrogenmaleate form from ethanol/diethyl ether

Sources & evidence

ORD record
ord-adca1c80bf37432094417255893383ad
Source dataset
uspto-grants-1998_01
Patent number
US05708171

Reaction notes

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