HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 54517905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611560 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54517905 | HCID 54517905 | 48% |
Reaction Steps
To a solution of 10.0 mg (0.0437 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole in 3.0 mL dichloromethane were added 6.2 mg (0.0874 mMol) methyl isothiocyanate. The reaction was mixed for 48 hours and to it were then added 0.15 gm (0.0874 mMol) aminomethylated polystyrene and the reaction mixed for an additional 18 hours. The reaction mixture was then filtered and the volatiles evaporated to give 6.3 mg (48%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05708187 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-85a87524a3b845318a612bfa795aaba5 |
| Source note | uspto-grants-1998_01 |