HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57284408, compound → HCID 70181628, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57284408 | HCID 57284408 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70181628 | HCID 70181628 | — |
Reaction Steps
The compound (0.578 g) obtained in the above (4) is dissolved in ethanol (15 ml), and thereto is added 10% palladium-carbon (50% wet, 0.4 g), and the mixture is stirred at room temperature for four hours under hydrogen atmosphere. The insoluble materials are removed by filtration, and the filtrate is concentrated under reduced pressure to give the title compound (398 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05707994 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-f2be43f1997e40c58fb264b4c5805079 |
| Source note | uspto-grants-1998_01 |