HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 1-methyl-4-nitro-1H-pyrrole-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Methyl 4-nitro-1h-pyrrole-2-carboxylate | HCID 261887 | — |
| Product | Methyl 1-methyl-4-nitro-1H-pyrrole-2-carboxylate | HCID 2759930 | 89% |
Reaction Steps
Following the basic procedure of Example 25(d), by reacting 2.9 g (17 mmol) of methyl 4-nitro-2-pyrrolecarboxylate with 1.1 ml of iodomethane, 2.8 g (89%) of the expected compound of melting point 122°-124° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05709867 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-2fbddfa821b84ea3a3d13c2a3e429680 |
| Source note | uspto-grants-1998_01 |