HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 178496926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Amino-4,5-dichlorobenzaldehyde | HCID 818013 | — |
| Reactant | Dimethylmalonat | HCID 6946994 | — |
| Product | HCID 178496926 | HCID 178496926 | — |
Reaction Steps
3,4-Dichloro-6-aminobenzaldehyde (2.85 g, 15 mmol) was stirred with dimethylmalonate (10 ml) at 140° C. for 20 h. The mixture was diluted with ethyl ether (100 ml). The precipitate was collected, washed twice with ethyl ether and dried in vacuo to give 2.86 g of methyl 6,7-dichloro-2-hydroxyquinoline-3-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05710139 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-23d4d49596454dcd92078d9946d5b5ab |
| Source note | uspto-grants-1998_01 |