HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 10769056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | o-Phenylbenzoic acid | HCID 70357 | — |
| Reactant | HCID 10666969 | HCID 10666969 | — |
| Product | HCID 10769056 | HCID 10769056 | 96.7% |
Reaction Steps
Using 127 mg of o-phenylbenzoic acid, 0.141 ml of oxalyl chloride and 200 mg of methyl (E)-[1-(4-aminobenzoyl)-4,4-difluoro-2,3,4,5-tetrahydro-1H-1-benzazepin-5ylidene]acetate, a similar procedure as in Reference Example 8 was repeated to obtain 287 mg of methyl (E)-[4,4-difluoro-1-[4-(2-phenylbenzoylamino)benzoyl]-2,3,4,5-tetrahydro-1H-1-benzazepin-5-ylidene]acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05710150 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-e52d8b2f7f304df0826cad163113b262 |
| Source note | uspto-grants-1998_01 |