1-(6'-oxoheptyl)-3,7-dimethylxanthine → HCID 10565738, compound

HRID 726794Notes

Reaction equation

HRID 726794 reaction equation
[O:1]=[C:2]([CH3:21])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:17](=[O:18])[C:16]2[N:15]([CH3:19])[CH:14]=[N:13][C:12]=2[N:11]([CH3:20])[C:9]1=[O:10].[BH4-].[Na+]>>[OH:1][CH:2]([CH3:21])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][N:8]1[C:17](=[O:18])[C:16]2[N:15]([CH3:19])[CH:14]=[N:13][C:12]=2[N:11]([CH3:20])[C:9]1=[O:10]

Participants

3

Reactant 2

HCID 5253351-(6'-oxoheptyl)-3,7-dimethylxanthineHCID 4311764Sodium borohydride

Product 1

HCID 10565738HCID 10565738, compound

Procedure

Racemic 1-(6-hydroxyheptyl)-3,7-dimethylxanthine (melting point: 76°-77° C.) was prepared for comparison by reduction of 1-(6-oxoheptyl)-3,7-dimethylxanthine with NaBH4 analogously to d).

Sources & evidence

ORD record
ord-9d3176f222614bd7827749a1bf47ef00
Source dataset
uspto-grants-1998_01
Patent number
US05710272

Reaction notes

Loading…