Methylamine → HCID 86751971, compound

Participants

Reaction Steps

2 ml of 33% methylamine solution (in ethanol) are added to a solution of 1.02 g of 2-(2-methylphenoxymethyl)-phenylglyoxalic acid methyl ester O-fluoromethyl oxime in 30 ml of methanol and the reaction mixture is left to stand for 24 hours. Concentration by evaporation is then carried out in vacuo and the concentrate is crystallised from hexane. Pure 2-(2-methylphenoxymethyl)-phenylglyoxalic acid N-methylamide O-fluoromethyl oxime is obtained; m.p. 86°-88° C.

Provenance & Evidence