HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 19707486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 19707491 | HCID 19707491 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19707486 | HCID 19707486 | — |
Reaction Steps
To a solution of the product from Step 2 (360 mg, 1.28 mmol) in 10 mL of THF at room temperature was added water (0.025 mL), followed by triphenylphosphine (364 mg, 1.41 mmol). The solution was stirred at room temperature. After 84 hours, the reaction was concentrated in vacuo to provide the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05710171 |
| Source dataset | uspto-grants-1998_01 |
| ORD ID | ord-c7aeb4776e364022aa7386952b72e84c |
| Source note | uspto-grants-1998_01 |