HCID 19705213, compound → HCID 19705279, compound

HRID 727183Notes

Reaction equation

HRID 727183 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]([CH:11]2[CH2:16][CH2:15][C:14](=[O:17])[CH2:13][CH2:12]2)([CH3:10])[CH3:9])[CH:5]=[CH:6][CH:7]=1>[Pd].C(O)C>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]([C:11]2[CH2:16][CH2:15][C:14](=[O:17])[CH2:13][CH:12]=2)([CH3:9])[CH3:10])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 1

HCID 19705213HCID 19705213, compound

Product 1

HCID 19705279HCID 19705279, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

This compound is prepared in a manner analogous to that of Step C of Example 2, by the hydrogenation of 6.5 grams (0.026 mole) of 1-[2-(3-chlorophenyl)propan-2-yl]-1-cyclohexen-4-one in the presence of 0.4 gram (catalyst) of 10% palladium on charcoal in 50 mL of ethanol, yielding 4-[2-(3-chlorophenyl)propan-2-yl]cyclohexanone.

Workup

  1. customThis compound is prepared in a manner analogous to that of Step C of Example 2

Sources & evidence

ORD record
ord-c1b5ce31c8bf4ee2887b2c881a54cece
Source dataset
uspto-grants-1998_01
Patent number
US05712281

Reaction notes

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