Water → HCID 19705271, compound

HRID 727201Notes

Reaction equation

HRID 727201 reaction equation
[F:1][C:2]([F:22])([F:21])[C:3]1[CH:4]=[C:5]([CH2:9][O:10][CH:11]2[CH2:20][CH2:19][C:14]3(OCC[O:15]3)[CH2:13][CH2:12]2)[CH:6]=[CH:7][CH:8]=1.O>C(O)(=O)C>[F:1][C:2]([F:21])([F:22])[C:3]1[CH:4]=[C:5]([CH2:9][O:10][CH:11]2[CH2:12][CH2:13][C:14](=[O:15])[CH2:19][CH2:20]2)[CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 2

HCID 962WaterHCID 19705202HCID 19705202, compound

Product 1

HCID 19705271HCID 19705271, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

This compound is prepared in a manner analogous to that of Step D of Example 2, using 7.9 grams (0.025 mole) of 8-(3-trifluoromethylphenylmethoxy)-1,4-dioxaspiro[4.5]decane. and 25 mL of water in 50 mL of acetic acid, yielding 4-(3-trifluoromethylphenylmethoxy)cyclohexanone.

Workup

  1. customThis compound is prepared in a manner analogous to that of Step D of Example 2

Sources & evidence

ORD record
ord-69c20ac363894f76aab35d50bd75ad6f
Source dataset
uspto-grants-1998_01
Patent number
US05712281

Reaction notes

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