Acetyl chloride → HCID 22101836, compound

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Reaction Steps

Acetyl chloride was added to a solution of the product from Example 56 and triethylamine in dry dichloromethane. The mixture was stirred at room temperature overnight and then washed with aqueous sodium hydrogen carbonate solution. The organic phase was separated, dried and evaporated and the residue was purified by flash chromatography to give the title compound.

Provenance & Evidence