Methyl iodide → 131988-11-9

HRID 727280Notes

Reaction equation

HRID 727280 reaction equation
[CH3:1][I:2].[CH3:3][O:4][C:5]1[C:6]([C:10]2[CH:11]=[N:12][CH:13]=[CH:14][CH:15]=2)=[N:7][S:8][N:9]=1>CC(C)=O>[I-:2].[CH3:3][O:4][C:5]1[C:6]([C:10]2[CH:11]=[N+:12]([CH3:1])[CH:13]=[CH:14][CH:15]=2)=[N:7][S:8][N:9]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180130131987-61-6

Product 1

HCID 15819039131988-11-9

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.37 ml, 6 mmol) and 3-(4-methoxy-1,2,5-thiadiazol-3-yl)pyridine (500 mg, 2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration. Yield: 1.0 g (100%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-495daf9f3f804314ad212b8d27628376
Source dataset
uspto-grants-1998_01
Patent number
US05712297

Reaction notes

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