Methyl iodide → HCID 19075363, compound

HRID 727294Notes

Reaction equation

HRID 727294 reaction equation
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH:5]([CH3:7])[CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075319HCID 19075319, compound

Product 1

HCID 19075363HCID 19075363, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 10 mmol) and 3-(4-isopentyloxy-1,2,5-thiadiazol-3-yl)pyridine (622 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.78 g (81%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.78 g (81%)

Sources & evidence

ORD record
ord-54fb2b976f034d94843f9fa6b1dea719
Source dataset
uspto-grants-1998_01
Patent number
US05712297

Reaction notes

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