Methyl iodide → HCID 19705390, compound

HRID 727298Notes

Reaction equation

HRID 727298 reaction equation
[CH3:1][I:2].[CH2:3]([O:10][C:11]1[C:12]([C:16]2[CH:17]=[N:18][CH:19]=[CH:20][CH:21]=2)=[N:13][S:14][N:15]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1>CC(C)=O>[I-:2].[CH2:3]([O:10][C:11]1[C:12]([C:16]2[CH2:17][N:18]([CH3:1])[CH:19]=[CH:20][CH:21]=2)=[N:13][S:14][N:15]=1)[C:4]1[CH:5]=[CH:6][CH:7]=[CH:8][CH:9]=1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075281HCID 19075281, compound

Product 1

HCID 19705390HCID 19705390, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(4-benzyloxy-1,2,5-thiadiazol-3-yl)pyridine (673 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.75 g (73%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.75 g (73%)

Sources & evidence

ORD record
ord-d936bf3891124161b3e0f178c72e822a
Source dataset
uspto-grants-1998_01
Patent number
US05712297

Reaction notes

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