Methyl iodide → 3-(3-(2-(2-Methoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-Yl)-1-methylpyridinium iodide

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Reaction Steps

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(4-(2-(2-methoxyethoxy)ethoxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.76 g (60%).

Provenance & Evidence