Methyl iodide → HCID 19075251, compound

HRID 727356Notes

Reaction equation

HRID 727356 reaction equation
[CH3:1][I:2].[CH2:3]([S:6][C:7]1[C:8]([C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH2:4][CH3:5]>CC(C)=O>[I-:2].[CH2:3]([S:6][C:7]1[C:8]([C:12]2[CH:13]=[N+:14]([CH3:1])[CH:15]=[CH:16][CH:17]=2)=[N:9][S:10][N:11]=1)[CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180155HCID 15180155, compound

Product 1

HCID 19075251HCID 19075251, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(4-propylthio-1,2,5-thiadiazol-3-yl)pyridine (0.63 g, 2.6 mmol) in acetone (5 ml) was stirred at room temperature for 18 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-09586f9f067b4ea4ba0cb8109590759d
Source dataset
uspto-grants-1998_01
Patent number
US05712297

Reaction notes

Loading…