Methyl iodide → HCID 19705377, compound

HRID 727358Notes

Reaction equation

HRID 727358 reaction equation
[CH3:1][I:2].[CH2:3]([S:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH2:5][CH3:6]>>[I-:2].[CH2:3]([S:7][C:8]1[C:9]([C:13]2[CH2:14][N:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 10729454HCID 10729454, compound

Product 1

HCID 19705377HCID 19705377, compound

Procedure

Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(4-butylthio-1,2,5-thiadiazol-3-yl)pyridine (0.6 g, 2.3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-ed7fcbfc636e496296163a798b28e4dd
Source dataset
uspto-grants-1998_01
Patent number
US05712297

Reaction notes

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