Methyl iodide → HCID 19075235, compound

HRID 727372Notes

Reaction equation

HRID 727372 reaction equation
[CH3:1][I:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N:17][CH:18]=[CH:19][CH:20]=2)=[N:12][O:13][N:14]=1)[CH2:4][C:5]#[C:6][CH2:7][CH3:8]>CC(C)=O>[I-:2].[CH2:3]([O:9][C:10]1[C:11]([C:15]2[CH:16]=[N+:17]([CH3:1])[CH:18]=[CH:19][CH:20]=2)=[N:12][O:13][N:14]=1)[CH2:4][C:5]#[C:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075258HCID 19075258, compound

Product 1

HCID 19075235HCID 19075235, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (1.5 ml, 22 mmol) and 3-(4-(3-hexynyloxy)-1,2,5-oxadiazol-3-yl)pyridine (2.5 mmol) in acetone (20 ml) was stirred at room temperature for 18 h and evaporated to give the title compound.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-34ea98e1fcae4cfab248c06d9aca927c
Source dataset
uspto-grants-1998_01
Patent number
US05712297

Reaction notes

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