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HRID727657

反应详情

EQUATION

反应方程式

HRID 727657 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(CS[C@H]2C[C@@H](C(=O)N[C@@H]3CCNC3)N(C(=O)OCc3ccc([N+](=O)[O-])cc3)C2)cc1.Cl
HCID67586513

未命名化合物

结构：CC(=N)NC(=O)OCc1ccc([N+](=O)[O-])cc1
HCID140352007

未命名化合物

PRODUCTS

生成物

1
结构：CC(=NC(=O)OCc1ccc([N+](=O)[O-])cc1)N1CC[C@@H](NC(=O)[C@@H]2C[C@H](S)CN2C(=O)OCc2ccc([N+](=O)[O-])cc2)C1
HCID88299617

未命名化合物

收率 53.1%

PROCEDURE

实验过程

Following a procedure similar to that described in Preparation 23(iii) and 23(iv), but using 0.76 g of (2S,4S)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)-2-[(3R)-pyrrolidin-3-ylaminocarbonyl]pyrrolidine hydrochloride and 0.33 g of N-(4-nitrobenzyloxycarbonyl)acetamidine, 0.45 g of the title compound was obtained as a powder.