HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14455969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Tosylmethyl isocyanide | HCID 161915 | — |
| Reactant | HCID 54310861 | HCID 54310861 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 14455969 | HCID 14455969 | — |
Reaction Steps
N-Benzylidene-N',N'-dimethylsulphamide (6.36 g) was stirred with p-toluenesulphonylmethyl isocyanide (9.75 g ) and potassium carbonate (8.28 g) in methanol and dimethoxyethane for 18 hours. The mixture was filtered and the filtrate evaporated and recrystallised from ethyl acetate/hexane to give crude 1-dimethylsulphamoyl-5-phenylimidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05045557 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-2e2347db0dc34c16bfefa39882822b1f |
| Source note | uspto-grants-1991_09 |