HCID 67928382, compound → HCID 131716998, compound

HRID 727944Notes

Reaction equation

HRID 727944 reaction equation
C(O)(=O)C(O)=[O:3].[CH2:7]([O:9][CH2:10][CH2:11][O:12][C:13]1[CH:31]=[CH:30][C:16]([CH2:17][CH2:18][NH:19]CC(C2C=CC=CC=2)CO)=[CH:15][CH:14]=1)[CH3:8]>CS(C)=O>[CH2:7]([O:9][CH2:10][CH2:11][O:12][C:13]1[CH:31]=[CH:30][C:16]([CH2:17][C:18]([NH2:19])=[O:3])=[CH:15][CH:14]=1)[CH3:8]

Participants

3

Reactant 1

HCID 67928382HCID 67928382, compound

Product 1

HCID 131716998HCID 131716998, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

from N-[(R or S)-3-hydroxy-2-phenylpropyl]-p-(2-ethoxyethoxy)phenylacetamide there was prepared (R or S)-β-[[[p-(2-ethoxyethoxy)phenethyl]amino]methyl]-phenethyl alcohol oxalate m.p. 152°-154° C., [α]D -9° (DMSO, c=1%)

Sources & evidence

ORD record
ord-1e744af8eaef4a2ba261df4f418769a0
Source dataset
uspto-grants-1991_09
Patent number
US05045567

Reaction notes

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