HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 13873005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2,4-Dibenzyloxybenzyl Alcohol | HCID 10567710 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13873005 | HCID 13873005 | — |
Reaction Steps
2,4-Dibenzyloxybenzyl alcohol (19.8 g) was dissolved in anhydrous benzene (150 ml) and then thereto was added thionyl chloride (40 g), followed by reflux under heating for 1 hour. This was concentrated to dryness under reduced pressure to obtain crude 2,4-dibenzyloxybenzyl chloride. This product was used for the subsequent reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047430 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-bc7511e8ca7a481db005d0bacd6ceb6d |
| Source note | uspto-grants-1991_09 |