HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-methylpyridine → HCID 54521931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-methylpyridine | HCID 1533 | — |
| Reactant | HCID 54548024 | HCID 54548024 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 54521931 | HCID 54521931 | 55.8% |
Reaction Steps
A mixture of 4-bromo-1-(4-nitrophenyl)but-1-en-3-one (5.7 g) and 2-amino-4-methylpyridine (6.8 g) in acetonitrile (50 ml) was stirred under reflux for 1.5 hours. The precipitate was collected by filtration and washed with acetonitrile to give 2-[2-(4-nitrophenyl)vinyl]-7-methylimidazo[1,2-a]pyridine (3.29 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047411 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-6d4fe4b3fc914b31b236a0cd4220a866 |
| Source note | uspto-grants-1991_09 |