Methyl isothiocyanate → HCID 10377776, compound

Participants

Reaction Steps

A solution of 2-(4-aminobenzyl)pyridine (3.8 g) and methyl isothiocyanate (2.0 g) in ethanol (100 ml) was heated under reflux for 2 hours. Evaporation of the solvent gave a residue which was triturated with diethyl ether to give a precipitate. The precipitate was collected by filtration and dried to give 2-[4-(3-methylthioureido)benzyl]pyridine (4.11 g).

Provenance & Evidence