HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 15171499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 15171488 | HCID 15171488 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15171499 | HCID 15171499 | 94.3% |
Reaction Steps
A solution of 3-(3-amino-4-hydroxybenzyl)-2,7-dimethylimidazo[1,2-a]pyridine (3.1 g) and ethyl isocyanate (1.24 g) in ethanol (50 ml) and tetrahydrofuran (50 ml) was refluxed for 2.5 hours under stirring. The reaction mixture was concentrated in vacuo and the precipitate was collected by filtration to give 3-[3-(3-ethylureido)-4-hydroxybenzyl]-2,7-dimethylimidazo[1,2-a]pyridine (3.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047411 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-8fec09af7b1a4b7390f7525f4c08e6df |
| Source note | uspto-grants-1991_09 |