HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 178436799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 1-Ethyl-9-methylphenothiazin-5-ium tetraiodide hydrate | HCID 86667030 | — |
| Product | HCID 178436799 | HCID 178436799 | — |
Reaction Steps
To the stirred mixture of 1-ethyl-9-methylphenothiazin-5-ium tetraiodide hydrate (383 mg, 0.5 mmol) in anhydrous CHCl3 (20 mL) dimethylamine (0.5 mL, 1.0 mmol, 2 M solution in THF) was added drop wise over 4 h. The resulting mixture was stirred at room temperature overnight, concentrated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08828986B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-f5a17d5163fa4d7fbc340b8627ac579a |
| Source note | uspto-grants-2014_09 |