Iodoethane → HCID 67930823, compound

Participants

Reaction Steps

The title compound was prepared from 1,6-anhydro-4-O-benzyl-2-O-methyl-β-D-allopyranose (0.135 g) (see Example 29) in the same way as described for the 3-O-methyl analogue (see Example 30) but employing ethyl iodide (0.624 g) instead of methyl iodide. It was obtained as a colourless oil (0.089 g); 1H-nmr data: 7.2-7.5 (m, Ph), 5.6 (d, H-1), 4.8 (m, PhCH2O), 4.55 (m, H-5), 1.25 (t, CH2CH3), and 3.4-3.7 (m, remaining protons).

Provenance & Evidence