HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 19824106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 12-Aminododecanoic Acid | HCID 69661 | — |
| Reactant | N-Hydroxysuccinimide | HCID 80170 | — |
| Reactant | 11-iodoundecanoic Acid | HCID 11461104 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19824106 | HCID 19824106 | 84% |
Reaction Steps
Similar to example 2, reaction of 07.90 g (25.3 mmol) 11-iodoundecanoic acid with 2.90 g (25.3 mmol) N-hydroxysuccinimide and 5.22 g (25.3 mmol) DCC gave 10.0 g (96%) of the succiminidylester, which was reacted with 5.40 g (25.1 mmol) 12-aminododecanoic acid to yield 10.5 g (84%) of colourless crystals, m.p. 107°-110° C. (methanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047535 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-bdc95e64a2924b17a444f8d7f5dab5b6 |
| Source note | uspto-grants-1991_09 |