反应详情

温度

50 °C

To a solution 3,7-bis-morpholino-1-fluoro-10-Boc-phenothiazine (122 mg) in dichloromethane (10 mL) HCl (2 mL, 4 M solution in 1,4-dioxane)) was added. The reaction mixture was stirred at 50° C. for 3 h. Solvent was removed under vacuum. Product was purified by flash chromatography and prep-chromatography.

1. customSolvent was removed under vacuum
2. customProduct was purified by flash chromatography and prep-chromatography