Chloroform → 129904-55-8

HRID 728322Notes

Reaction equation

[N+:1]([O:4][CH2:5][CH2:6][CH2:7][O:8][C:9]([C:11]1[CH:12]([C:33]2[CH:38]=[CH:37][CH:36]=[C:35]([N+:39]([O-:41])=[O:40])[CH:34]=2)[C:13]([C:19]([O:21][CH2:22][CH2:23][NH:24][C:25](=[O:32])[C:26]2[CH:31]=[CH:30][CH:29]=[N:28][CH:27]=2)=[O:20])=[C:14]([CH3:18])[NH:15][C:16]=1[CH3:17])=[O:10])([O-:3])=[O:2].C(Cl)(Cl)[Cl:43]>>[ClH:43].[N+:1]([O:4][CH2:5][CH2:6][CH2:7][O:8][C:9]([C:11]1[CH:12]([C:33]2[CH:38]=[CH:37][CH:36]=[C:35]([N+:39]([O-:41])=[O:40])[CH:34]=2)[C:13]([C:19]([O:21][CH2:22][CH2:23][NH:24][C:25](=[O:32])[C:26]2[CH:31]=[CH:30][CH:29]=[N:28][CH:27]=2)=[O:20])=[C:14]([CH3:18])[NH:15][C:16]=1[CH3:17])=[O:10])([O-:3])=[O:2]

Participants

Reactant 2

HCID 6212Chloroform

HCID 179845HCID 179845, compound

Product 1

HCID 179844129904-55-8

Procedure

Into a solution of Compound 2 in chloroform was introduced hydrogene chloride gas, and evaporation of the solvent under reduced pressure gave the title compound.

Workup

customchloride gas, and evaporation of the solvent under reduced pressure

Sources & evidence

ORD record: ord-be1896fd6e3248778ae75bc43f32d025
Source dataset: uspto-grants-1991_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05047543

Reaction notes

Loading…