1-Hexadecylthio-3-(3-iodopropylsulfonylamino)-2-methoxypropane → HCID 15667302, compound

HRID 728475Notes

Reaction equation

HRID 728475 reaction equation
Cl[CH2:2][CH2:3][CH2:4][S:5]([NH:8][CH2:9][CH:10]([O:34][C:35]1[CH:39]=[CH:38][O:37][N:36]=1)[CH2:11][O:12][C:13](=[O:33])[NH:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])(=[O:7])=[O:6].C(SCC(OC)CNS(CCC[I:67])(=O)=O)CCCCCCCCCCCCCCC>>[I:67][CH2:2][CH2:3][CH2:4][S:5]([NH:8][CH2:9][CH:10]([O:34][C:35]1[CH:39]=[CH:38][O:37][N:36]=1)[CH2:11][O:12][C:13](=[O:33])[NH:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])(=[O:7])=[O:6]

Participants

3

Reactant 2

HCID 148350231-Hexadecylthio-3-(3-iodopropylsulfonylamino)-2-methoxypropaneHCID 15667301HCID 15667301, compound

Product 1

HCID 15667302HCID 15667302, compound

Procedure

3-(3-Chloropropylsulfonylamino)-2-(3-isoxazolyloxy)-1-octadecylcarbamoyloxypropane IIIj2 is allowed to react and worked up by the same procedure as described in (5). m.p. 69°-71.5° C. The summary of the experimental condition and the physical data of the product are listed in Table 8.

Workup

  1. customto react

Sources & evidence

ORD record
ord-1bb50c51c8734cfd8c36c366940e6bd3
Source dataset
uspto-grants-1991_09
Patent number
US05047540

Reaction notes

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