3-Hexadecylthio-2-methoxymethylpropylamine → 3-(3-Chloropropylsulfonylamino)-1-hexadecylthio-2-methoxymethylpropane

HRID 728480Notes

Reaction equation

HRID 728480 reaction equation
[CH2:1]([S:17][CH2:18][CH:19]([CH2:22][O:23][CH3:24])[CH2:20][NH2:21])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[Cl:25][CH2:26][CH2:27][CH2:28][S:29](NCC(OC)CSCCCCCCCCCCCCCCCC)(=[O:31])=[O:30]>>[Cl:25][CH2:26][CH2:27][CH2:28][S:29]([NH:21][CH2:20][CH:19]([CH2:22][O:23][CH3:24])[CH2:18][S:17][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])(=[O:31])=[O:30]

Participants

3

Reactant 2

HCID 148350103-Hexadecylthio-2-methoxymethylpropylamineHCID 14835022HCID 14835022, compound

Product 1

HCID 148350753-(3-Chloropropylsulfonylamino)-1-hexadecylthio-2-methoxymethylpropane

Procedure

3-Hexadecylthio-2-methoxymethylpropylamine IVk3 is allowed to react and worked up by the same procedure as described in (4). m.p. 41.5°-43° C. The summary of the experimental and the physical data of the product are listed in Table 7.

Workup

  1. customto react

Sources & evidence

ORD record
ord-1c0b112380484d55ae0241c977e11ebf
Source dataset
uspto-grants-1991_09
Patent number
US05047540

Reaction notes

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