HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 14835079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 14835074 | HCID 14835074 | — |
| Reactant | HCID 14835078 | HCID 14835078 | — |
| Product | HCID 14835079 | HCID 14835079 | 85% |
Reaction Steps
A mixture of 0.72 g (1.1 mM) of 3-(3-iodopropylsulfonylamino)-2-methoxymethyl-1-octadecylcarbamoyloxypropane IIk2, 88 μl (1.2 mM) of acetyl chloride and 0.25 ml (1.4 mM) of N,N-diisopropylethylamine is allowed to react by the same procedure as described in (110) and 0.65 g (85% yield) of the title compound IIk2' is obtained. m.p. 71°-72° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047540 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-d361041d7e974dbf94850b18a7bef2b2 |
| Source note | uspto-grants-1991_09 |