2-Cyanomethyl-3-hexadecyloxypropylamine → 1-(3-Chloropropylsulfonylamino)-2-cyanomethyl-3-hexadecyloxypropane

HRID 728499Notes

Reaction equation

HRID 728499 reaction equation
[C:1]([CH2:3][CH:4]([CH2:7][O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:5][NH2:6])#[N:2].[Cl:25][CH2:26][CH2:27][CH2:28][S:29](NCC(OC)CSCCCCCCCCCCCCCCCC)(=[O:31])=[O:30]>>[Cl:25][CH2:26][CH2:27][CH2:28][S:29]([NH:6][CH2:5][CH:4]([CH2:3][C:1]#[N:2])[CH2:7][O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])(=[O:31])=[O:30]

Participants

3

Reactant 2

HCID 148350132-Cyanomethyl-3-hexadecyloxypropylamineHCID 14835022HCID 14835022, compound

Product 1

HCID 148350841-(3-Chloropropylsulfonylamino)-2-cyanomethyl-3-hexadecyloxypropane

Procedure

The crude 2-cyanomethyl-3-hexadecyloxypropylamine IVn1 prepared above is allowed to react by the same procedure as described in (4). The summary of the experimental condition and the physical data of the product are listed in Table 7.

Workup

  1. customto react by the same procedure

Sources & evidence

ORD record
ord-82b0b77dc6bc4fc9987b188eee1b0527
Source dataset
uspto-grants-1991_09
Patent number
US05047540

Reaction notes

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