HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Cyanide → 2-Cyanomethyl-3-octadecylcarbamoyloxypropyl benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | 2-Bromomethyl-3-n-octadecylcarbamoyloxypropyl benzoate | HCID 53884469 | — |
| Reactant | 2-Cyanomethyl-3-hexadecyloxypropyl benzoate | HCID 54541187 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-Cyanomethyl-3-octadecylcarbamoyloxypropyl benzoate | HCID 54117556 | 95.5% |
Reaction Steps
A mixture of 1.76 g (3.10 mM) of 2-bromomethyl-3-n-octadecylcarbamoyloxypropyl benzoate, 185 mg (3.26 mM) of 95% sodium cyanide in 30 ml of dimethylsulfoxide is allowed to react by the same procedure as described in the (136) and 1.49 g (95.5% yield) of the titled compound n5' is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047540 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-c2a24b7fd029413e8c77dc182d89261c |
| Source note | uspto-grants-1991_09 |