HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Benzoyloxypropan-1-yl)-3-octadecylcarbamoyloxypropylamine → 2-(2-Benzoyloxypropan-1-yl)-3-hexadecylthiopropylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Benzoyloxypropan-1-yl)-3-octadecylcarbamoyloxypropylamine | HCID 14835012 | — |
| Reactant | 1-Azido-2-(2-benzoyloxypropan-1-yl)-3-hexadecylthiopropane | HCID 19884195 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(2-Benzoyloxypropan-1-yl)-3-hexadecylthiopropylamine | HCID 14835015 | — |
Reaction Steps
A mixture of 1.291 g (2.56 mM) of 1-azido-2-(2-benzoyloxypropan-1-yl)-3-n-hexadecylthiopropane m12b, 130 mg of 10% palladium on charcoal in 130 ml of methanol is hydrogenated by the same procedure as described in (129) and crude product of the titled compound m13 is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05047540 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-ee2bca900bef4d33b6de21bdfd79d026 |
| Source note | uspto-grants-1991_09 |