Dichloromethane → HCID 14324551, compound

Participants

Reaction Steps

800 g of 3-nitro-4-chlorobenzenesulfonyl chloride and 1,000 ml of dichloromethane were mixed, and thereto was added dropwise a dichloromethane solution containing 600 g of hexadecylamine and 251 ml of triethylamine. After the completion of the reaction, the solvent used was distilled away under reduced pressure, and the residue was dissolved under heating in 3,000 ml of ethanol. Upon gradual cooling, crystals separated out. These crystals were filtered off, and dried. Yield: 1,020 g, Percent yield: 88%, Melting point: 91°-93° C.

Provenance & Evidence