HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Butyric acid [1-(6-methyl-2,3-dihydro-2-pyranyl)ethylidene]hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Butyrohydrazide | HCID 77079 | — |
| Reactant | Ethanone, 1-(3,4-dihydro-6-methyl-2H-pyran-2-yl)- | HCID 141413 | — |
| Solvent | Water | HCID 962 | — |
| Product | Butyric acid [1-(6-methyl-2,3-dihydro-2-pyranyl)ethylidene]hydrazide | HCID 131717001 | 12% |
Reaction Steps
A mixture of 5.0 gm (0.0356 mole) of 2-acetyl-6-methyl-2,3-dihydropyran, 3.64 gm (0.0356 mole) of n-butyric acid hydrazide and 100 ml of ethanol is refluxed 24 hr. The mixture is diluted with water to the cloud point and chilled. The product is collected, washed with water and dried to give 0.93 gm (12%) of the title compound having a melting point of 72.8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05049561 |
| Source dataset | uspto-grants-1991_09 |
| ORD ID | ord-f5ee7a77cb3648eeaa26c629764f2bdb |
| Source note | uspto-grants-1991_09 |