HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-oxocyclohexyl)acetic Acid → 2-(4-Hydroxy-4-methylcyclohexyl)acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-oxocyclohexyl)acetic Acid | HCID 9920438 | — |
| Reactant | HCID 178418689 | HCID 178418689 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(4-Hydroxy-4-methylcyclohexyl)acetic acid | HCID 51051673 | — |
Reaction Steps
Prepared using an excess of MeMgBr (26 mmol) in THF (20 ml) with (4-Oxo-cyclohexyl)-acetic acid (13 mmol) as described on Journal of American Society 93 (1), 1971, 121-129.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08829029B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-9c0abc16bb574c42ba9e4d3b1cac9333 |
| Source note | uspto-grants-2014_09 |