p-Toluenesulfonic acid → HCID 54530313, compound

Participants

Reaction Steps

A mixture of hydroxyethyl acrylate (11.6 g), an equivalent amount of 2-ethylenyl-5,5-dimethyl-1,3-dioxane (EDD) (14.2 g), and a catalytic amount of p-toluenesulfonic acid (100 mg) was heated at 65° C. overnight. Gas chromatography showed that reaction occurred. The unreacted starting materials were removed at 40° C. under 0.05 mm Hg.

Provenance & Evidence