2-Nitrobenzaldehyde → HCID 53747035, compound

HRID 728776Notes

Reaction equation

[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[CH2:12]2.[N+:19]([C:22]1[CH:29]=[CH:28][CH:27]=[CH:26][C:23]=1[CH:24]=O)([O-:21])=[O:20]>>[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[CH:24][C:23]1[CH:26]=[CH:27][CH:28]=[CH:29][C:22]=1[N+:19]([O-:21])=[O:20]

Participants

Reactant 2

HCID 111012-Nitrobenzaldehyde

HCID 13689754HCID 13689754, compound

Product 1

HCID 53747035HCID 53747035, compoundYield 33%

Procedure

Starting from 5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-1,3-dihydro-2H-indol-2-one and 2 nitro benzaldehyde and following the method described in Example 10, the desired compound was obtained.

Sources & evidence

ORD record: ord-3b9393dbf9874c90a7ea3a444f99bb65
Source dataset: uspto-grants-1991_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05051417

Reaction notes

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