Benzylhydrazine dihydrochloride → HCID 178435132, compound

HRID 728780Notes

Reaction equation

HRID 728780 reaction equation
[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[N:19]C1C=CC=CC=1.Cl.Cl.[CH2:28]([NH:35]N)[C:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1>>[C:29]1([CH2:28][NH:35][N:19]=[C:12]2[C:11]3[C:15](=[CH:16][CH:17]=[C:9]([C:3]4[CH:2]([CH3:1])[S:7][C:6](=[O:8])[NH:5][N:4]=4)[CH:10]=3)[NH:14][C:13]2=[O:18])[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1

Participants

3

Reactant 2

HCID 146540Benzylhydrazine dihydrochlorideHCID 1357781391,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one

Product 1

HCID 178435132HCID 178435132, compoundYield 24%

Procedure

Starting from 1,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo -2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one, and benzylhydrazine dihydrochloride and following the method described in Example 21, the desired compound was obtained.

Sources & evidence

ORD record
ord-dc5eced4399c45f490ca4cfab12bb2af
Source dataset
uspto-grants-1991_09
Patent number
US05051417

Reaction notes

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