4-Tert-butylphenylhydrazine hydrochloride → HCID 178435129, compound

HRID 728781Notes

Reaction equation

HRID 728781 reaction equation
[CH3:1][CH:2]1[S:7][C:6](=[O:8])[NH:5][N:4]=[C:3]1[C:9]1[CH:10]=[C:11]2[C:15](=[CH:16][CH:17]=1)[NH:14][C:13](=[O:18])[C:12]2=[N:19]C1C=CC=CC=1.Cl.[C:27]([C:31]1[CH:36]=[CH:35][C:34]([NH:37]N)=[CH:33][CH:32]=1)([CH3:30])([CH3:29])[CH3:28]>>[CH3:30][C:27]([C:31]1[CH:32]=[CH:33][C:34]([NH:37][N:19]=[C:12]2[C:11]3[C:15](=[CH:16][CH:17]=[C:9]([C:3]4[CH:2]([CH3:1])[S:7][C:6](=[O:8])[NH:5][N:4]=4)[CH:10]=3)[NH:14][C:13]2=[O:18])=[CH:35][CH:36]=1)([CH3:28])[CH3:29]

Participants

3

Reactant 2

HCID 162174584-Tert-butylphenylhydrazine hydrochlorideHCID 1357781391,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo-2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one

Product 1

HCID 178435129HCID 178435129, compoundYield 83%

Procedure

Starting from 1,3-dihydro-5-(3,6-dihydro-6-methyl-2-oxo -2H-1,3,4-thiadiazin-5-yl)-3-phenylimino-2H-indol-2-one, and 4t-butyl phenylhydrazine hydrochloride and following the method described in Example 21, the desired compound was obtained.

Sources & evidence

ORD record
ord-fc29e6749d024409960b18c765ecab01
Source dataset
uspto-grants-1991_09
Patent number
US05051417

Reaction notes

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